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溶剂热法直接合成酞菁铜晶体

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Indexed by:期刊论文

Date of Publication:2008-02-10

Journal:高等学校化学学报

Included Journals:SCIE、PKU、ISTIC、CSCD

Volume:29

Issue:2

Page Number:244-246

ISSN No.:0251-0790

Key Words:溶剂热合成;酞菁铜;单晶;喹啉

Abstract:以喹啉为溶剂,在反应釜中将1,3-二异吲哚、钼酸铵和二水乙酸铜在喹啉中反应,降至室温后得到长10.5 mm针状的酞菁铜单晶,最佳的反应条件: 以10 mL喹啉为溶剂,于270 ℃反应8 h,产率为51.3%.

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