Release Time:2019-03-10  Hits:

Indexed by: Journal Article

Date of Publication: 2009-10-20

Journal: 合成化学

Included Journals: CSCD、ISTIC、PKU

Volume: 17

Issue: 5

Page Number: 622-623,627

ISSN: 1005-1511

Key Words: 四氢硫芴;六氢硫芴;加氢脱硫;合成

Abstract: 以2-溴环己酮及苯硫酚为原料,经Tilak反应,然后环化合成了四氢硫芴(1);在三氟乙酸与锌粉存在下1于室温加氢制得六氢硫芴,其结构经1H NMR和GC-MS确证.