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Synthesis and characterization of multi-walled carbon nanotube doped silica aerogels

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Indexed by:期刊论文

Date of Publication:2012-06-01

Journal:JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION

Included Journals:SCIE、EI、ISTIC、Scopus

Volume:27

Issue:3

Page Number:512-515

ISSN No.:1000-2413

Key Words:multi-walled carbon nanotubes(MWCNT); silica aerogels; ambient pressure drying(APD)

Abstract:Multi-walled carbon nanotube doped silica aerogels(MWCNT-SAs) were synthesized from a wet gel of well-dispersed MWCNT by one-step solvent exchange/surface modification and ambient pressure drying(APD). Waterglass was employed as a precursor to prepare wet gel. The content of MWCNT varied from 0 to 15% volume by wet gel. The surface group, thermal stability and microstructure of pure silica aerogel and MWCNT-SAs were investigated by FTIR, DTA, and TEM. Experimental results show that MWCNT-SAs are hydrophobic when the temperature is below 400 A degrees C, MWCNT-SAs exhibit a mesoporous network structure, and they achieve the largest scale with least shrinkage and lowest density when doped with 5 vol% MWCNT.

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