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多羟基氮杂茋衍生物的化学合成

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Indexed by:期刊论文

Date of Publication:2022-06-29

Journal:应用化学

Affiliation of Author(s):化工学院

Issue:09

Page Number:117-119

ISSN No.:1000-0518

Abstract:One pyridine ring was introduced into the basic structure of stilbene in place of one of the benzene rings for the purpose of evaluating the activity change.Started from methoxyl substituted chloromethylpyridine,five new polyhydroxy-azastilbene-2-nitrogen derivatives(4a~4e) with(E)-isomer were synthesized via(Arbusow) reaction,Wittig-Horner reaction and demethalytion in a yield of 30%~34% as the main products.Their structures were characterized by IR,MS and ~(1)H NMR.

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