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论文类型：期刊论文

发表时间：2013-11-01

发表刊物：JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY

收录刊物：SCIE、EI、ISTIC、Scopus

卷号：29

期号：11

页面范围：1011-1017

ISSN号：1005-0302

关键字：Biomedical titanium alloy; alpha''-Martensite; Electron beam melting; Hardness; Optical and electron microscopy

摘要：Atomized, pre-alloyed Ti-24Nb-4Zr-7.9Sn (wt%) powder was used to fabricate solid, prototype components by electron beam melting (EBM). Vickers microindentation hardness values were observed to average 2 GPa for the precursor powder and 2.5 GPa for the solid, EBM-fabricated products. The powder and solid product microstructures were examined by optical and electron microscopy. X-ray diffraction analyses showed that they had bcc beta-phase microstructure. However, it was found by transmission electron microscopy that the EBM-fabricated product had plate morphology with space similar to 100-200 nm. Although the corresponding selected area diffraction patterns can be indexed by beta-phase plus alpha''-martensite with orthorhombic crystal structure, the dark-field analyses failed to observe the alpha''-martensite. Such phenomenon was also found in deformed gum metals and explained by stress-induced diffusion scattering due to phonon softening.