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溶剂热法直接合成酞菁铜晶体

Release Time:2019-03-10  Hits:

Indexed by: Journal Article

Date of Publication: 2008-02-10

Journal: 高等学校化学学报

Included Journals: CSCD、ISTIC、PKU、SCIE

Volume: 29

Issue: 2

Page Number: 244-246

ISSN: 0251-0790

Key Words: 溶剂热合成;酞菁铜;单晶;喹啉

Abstract: 以喹啉为溶剂,在反应釜中将1,3-二异吲哚、钼酸铵和二水乙酸铜在喹啉中反应,降至室温后得到长10.5 mm针状的酞菁铜单晶,最佳的反应条件: 以10 mL喹啉为溶剂,于270 ℃反应8 h,产率为51.3%.

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