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李晓杰
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研究员   博士生导师   硕士生导师

任职 : 爆炸技术研究所所长

性别: 男

毕业院校: 中国科学技术大学

学位: 博士

所在单位: 力学与航空航天学院

学科: 工程力学

办公地点: 力学楼224室

联系方式: 041184706163 科研之友主页: https://www.scholarmate.com/P/JzE7ru

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Detonation synthesis of TiO2/Na2Ti6O13powders

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论文类型: 会议论文

发表时间: 2021-07-21

卷号: 910 MSF

页面范围: 31-34

摘要: An easy and fast vacuum detonation method was designed to prepare TiO2/Na2Ti6O13powders. The mixed explosives, prepared by usage of Ti-Na-contained precursor, ammonium nitrate, hexogen and a certain mass of polystyrene foam ball (EPS) in beaker, were detonated in a vacuum detonation reactor to synthesize powders. The prepared light-grey powders were characterized by powder X-ray diffractometer and transmission electron microscopy to ascertain the phase composition and morphology. It was found that the powders were consisted of TiO2and Na2Ti6O13, and the TiO2almost was rutile phase. The intensity of Na2Ti6O13peak was enlarged with increase of EPS mass. The TiO2/Na2Ti6O13particles were irregular sphere or long rhombus, and some particles were 10 nm. In general, the dispersity of the powers was decreased with the mass of EPS increasing. © 2018 Trans Tech Publications, Switzerland.

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