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Hydrogen and Air Detonation (Deflagration) Synthesis of Carbon-Encapsulated Iron Nanoparticles

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Indexed by:Journal Papers

Date of Publication:2015-07-01

Journal:COMBUSTION EXPLOSION AND SHOCK WAVES

Included Journals:SCIE、EI、Scopus

Volume:51

Issue:4

Page Number:495-501

ISSN No.:0010-5082

Key Words:gaseous detonation; carbon-encapsulated iron nanoparticles; detonation tube; hydrogen; air

Abstract:With ferrocene as a precursor, carbon-encapsulated iron nanoparticles are synthesized through detonation of a gas mixture of hydrogen and air in a titanium detonation tube. XRD and TEM characterization shows that a downward trend in the size of particles can be observed with increasing amounts of the precursor. However, no further decrease occurs when the size of nanoparticles reaches approximately approximate to 40 nm, after which they remain in the range of 30-50 nm. The initial temperature of the detonation tube at 353 K is the optimal initial temperature for the synthesis. The average grain size of the synthesized products becomes larger as the temperature of detonation increases.

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