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论文类型:期刊论文
发表时间:2018-05-16
发表刊物:CHEMICAL PHYSICS LETTERS
收录刊物:SCIE、EI
卷号:700
页面范围:80-87
ISSN号:0009-2614
关键字:Initial saturation; Drying time; Adsorption; Sublimation-desorption;
Mass transfer
摘要:Freeze-drying of initially porous frozen material was investigated aimed at improving the process economics by reducing drying time and raising productivity. Experimental results showed that freeze-drying can be significantly enhanced by the frozen material with prebuilt porosity, and about 31% of drying time can be saved compared with the conventionally solid frozen material under the tested operating conditions. A multiphase transport model was formulated based on the local mass non-equilibrium assumption. Numerical results showed excellent agreements between measured and predicted drying curves. Analyses of saturation and temperature profiles displayed that volumetric sublimation-desorption can occur for the initially porous frozen material. (C) 2018 Elsevier B.V. All rights reserved.