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Preparation of diamond nanocrystals from catalysed carbon black in a high magnetic field

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Indexed by:期刊论文

Date of Publication:2003-11-26

Journal:JOURNAL OF PHYSICS-CONDENSED MATTER

Included Journals:Scopus、SCIE、EI

Volume:15

Issue:46

Page Number:8049-8054

ISSN No.:0953-8984

Abstract:Under a static high magnetic field of 10 T, diamond-like carbon (DLC) nanocrystals and graphite-coated n-diamond nanoparticles have been synthesized after a pyrogenation of carbon black and a nanometre-sized iron catalyst at atmospheric pressure and a temperature of 1100degreesC. The product is analysed by x-ray diffraction, Raman spectroscopy, transmission electron microscopy and electron-probe microanalysis. The average size of the DLC nanopowders is about 20 nm, and that of the graphite-coated n-diamond particles is about 100 nm. The yield of diamond is as high as 30%.

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