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Crystal Size Distribution and Aspect Ratio Control for Rodlike Urea Crystal via Two-Dimensional Growth Evaluation
Release time:2019-03-10 Hits:
Indexed by: 期刊论文
First Author: Li, Pan
Correspondence Author: Jiang, XB (reprint author), Dalian Univ Technol, R&D Ctr Membrane Sci & Technol, State Key Lab Fine Chem, Sch Chem Engn, Dalian 116024, Liaoning, Peoples R China.
Co-author: He, Gaohong,Lu, Dapeng,Xu, Xiaoyu,Chen, Shuo,Jiang, Xiaobin
Date of Publication: 2017-03-08
Journal: 251st National Meeting of the American-Chemical-Society (ACS)
Included Journals: SCIE、EI、CPCI-S
Document Type: J
Volume: 56
Issue: 9
Page Number: 2573-2581
ISSN No.: 0888-5885
Abstract: Research on the evaluation of the two characteristic dimensional parameters (crystal length and width) of rodlike urea crystals is proposed. The two-dimensional crystal growth and the corresponding crystal aspect ratios (AR) are highlighted during the evaluation. Various particle size analysis methods are then introduced to investigate two-dimensional growth mechanisms. Improved crystal morphology (varied from rodlike to columnar), crystal size distribution (coefficient of variation = 31.4), and AR (4.97) are obtained by the proposed operation profile (increasing cooling rate from 0.05 to 0.40 degrees C min(-1) and stable stirring rate of 300 rpm).
Translation or Not: no