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论文类型:期刊论文
发表时间:2012-01-15
发表刊物:MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES
MICROSTRUCTURE AND PROCESSING
收录刊物:SCIE、EI
卷号:532
页面范围:78-83
ISSN号:0921-5093
关键字:Polymer composites; Plasma; Interfaces; Aging; Humid resistance
摘要:In this study the radio frequency oxygen plasma was used to strengthen the interfacial adhesion of PBO fiber/bismaleimide composite. The interlaminar shear strength (ILSS) was improved to 57 MPa or by 29% after treatment at 50W, but higher powers reduced the adhesion. The fiber surface chemistry, topography and roughness were analyzed by XPS and AFM, respectively. Oxygen atoms and polar groups were increasingly introduced onto the fiber surface, which contributed much to better wettability. The fiber surface was roughened by plasma sputtering and etching, generating many protuberances and notches. Results suggested that physical interactions between the fiber and the matrix might play leading roles in strengthening the adhesion. Aging behavior was not observed within the storage time of 1-50 days, which indicated that the plasma created stable structures on the fiber surface. After boiling the ILSS retained above 90%, confirming that the composite had good resistance to humidity. (C) 2011 Elsevier BM. All rights reserved.