个人信息Personal Information
教授
博士生导师
硕士生导师
任职 : 建筑材料研究所所长、土木水利国家级实验教学中心常务副主任
性别:男
毕业院校:大连理工大学
学位:博士
所在单位:建设工程学院
学科:材料学. 结构工程. 市政工程
办公地点:大连理工大学3号实验楼
联系方式:0411-84707101
电子邮箱:wangbm@dlut.edu.cn
Modification of Ultraviolet Spectrophotometry Representational Method in Graphene Nanoplates Dispersion
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论文类型:期刊论文
发表时间:2020-07-01
发表刊物:JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY
收录刊物:PubMed、SCIE
卷号:20
期号:7
页面范围:4015-4022
ISSN号:1533-4880
关键字:Graphene Nanoplates (GNPs); Dispersion; UV Spectrophotometry; Modification
摘要:Graphene nanoplates (GNPs) are carbon nanomaterials with two-dimensional structure which is easy to reunite and their dispersion is necessary before using. The existing methods for dispersion characterization mainly include UV spectrophotometry, scanning electron microscope (SEM), transmission electron microscopy (TEM) and Atomic Force Microscopy (AFM). In this research study, sodium dodecyl benzene sulfonate (SOBS), polyoxyethylene (40) nonylphenyl ether, branched (C0890), polyvinyl pyrrolidone (PVP) and cetyltrimethyl ammonium bromide (CTAB) were used as dispersants, and ultrasonic treatment was employed as dispersion method. Ultraviolet spectrum for GNPs showed that some errors were attained, resulting from dispersant at 274 nm characteristic wavelength of GNPs dispersions with deionized water as controlled sample. The errors could be eliminated if dispersant solution was used as controlled sample. The microstructures of dispersed GNPs observed by SEM, TEM and AFM suggested that the GNPs were dispersed uniformly with 2.5 g/L SOBS, which showed the best dispersion effect. Raman spectrum indicated that more chaotic distribution and edge structures were achieved after dispersion.