点击次数：

论文类型：期刊论文

发表时间：2014-07-01

发表刊物：MATERIALS SCIENCE AND ENGINEERING B-ADVANCED FUNCTIONAL SOLID-STATE MATERIALS

收录刊物：SCIE、EI

卷号：185

期号：1

页面范围：129-133

ISSN号：0921-5107

关键字：Melamine; Functionalization; Microwave; Nitrogen-doped graphene

摘要：In this paper, we propose a solid microwave-mediated method for scalable production of nitrogen-doped graphene sheets (NGS) using low-cost industrial material melamine as functionalizing agent and nitrogen source. The strong interaction of microwaves with graphene oxide has been fully utilized to generate in situ heating that induces the decompose melamine and nitrogen doping of graphene. The morphology, structure, and components of the as-produced nitrogen-doped graphene are characterized by scanning electron microscopy (SEM), transmission electron microscope (TEM), Brunauer-Emmett-Teller (BET), pore-size distribution (PSD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectra (XPS), X-ray diffraction (XRD), and Raman spectroscopy. The results show NGS can be successfully synthesized via this strategy. (C) 2014 Elsevier B.V. All rights reserved.