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One-pot hydrothermal synthesis of mesoporous silica nanoparticles using formaldehyde as growth suppressant

发表时间:2019-03-09
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论文类型:
期刊论文
第一作者:
Gu, Lin
通讯作者:
Guo, XW (reprint author), Dalian Univ Technol, State Key Lab Fine Chem, PSU DUT Joint Ctr Energy Res, Sch Chem Engn, Dalian 116024, Peoples R China.
合写作者:
Zhang, Anfeng,Hou, Keke,Dai, Chengyi,Zhang, Shuguang,Liu, Min,Song, Chunshan,Guo, Xinwen
发表时间:
2012-04-01
发表刊物:
MICROPOROUS AND MESOPOROUS MATERIALS
收录刊物:
SCIE、EI、Scopus
文献类型:
J
卷号:
152
页面范围:
9-15
ISSN号:
1387-1811
关键字:
Mesoporous nanoparticles; Hydrothermal synthesis; Formaldehyde; Suppressed growth
摘要:
An effective one-pot hydrothermal synthesis method based on suppressed growth strategy was invented to produce mesoporous silica nanoparticles (MSNs). In a TEOS-CTAB-NH4OH-water-formaldehyde system, formaldehyde was used as suppressant which formed a polymer shell on the outer surface of the MSNs to control the particle size to about 30 nm. A nanoporous carbon framework was obtained when precursor was carbonized in N-2 followed by a HF leaching of the silica. The pore size of the carbon was about 30 nm. The mechanism for the synthesis process was described. (C) 2011 Elsevier Inc. All rights reserved.
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