肖义
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5,10,15,20-四(4-羟基苯基)卟啉的合成及光谱性质的研究
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Indexed by:期刊论文

Date of Publication:2006-10-25

Journal:染料与染色

Volume:43

Issue:5

Page Number:30-33

ISSN No.:1672-1179

Key Words:5,10,15,20-四(4-羟基苯基)卟啉;5,10,15,20-四(4-甲氧基苯基)卟啉;微波加热法;光谱性质

Abstract:以吡咯、对甲氧基苯甲醛和吡啶盐酸盐为原料,采用两步法合成了5,10,15,20-四(4-羟基苯基)卟啉(THPP),反应总收率39.2%,产品纯度大于97%;采用微波加热法提高了该产物的合成效率;用1HNMR、HPLC-MS和HRMS对化合物进行了结构和纯度表征;研究了其在不同溶剂和不同pH值条件下的光谱性质.

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Gender:Male

Alma Mater:Dalian University of Technology

Degree:Doctoral Degree

School/Department:State Key Laboratroy of Fine Chemicals

Discipline:Applied Chemistry. Fine Chemicals. Biochemical Engineering

Business Address:West Campus E-204

Contact Information:xiaoyi@dlut.edu.cn 0411-84986251

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