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Wei Zhang

Professor
Supervisor of Doctorate Candidates
Supervisor of Master's Candidates


Gender:Male
Alma Mater:University of Leeds
Degree:Doctoral Degree
School/Department:Department of Engineering Mechanics
Discipline:Engineering Mechanics
Biomechanics and Nanomechanics
Materials Physics and Chemistry
Business Address:Bldg.of Engineering Mechanics, Rm407
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Current position: Home >> Scientific Research >> Paper Publications
One-step synthesis of 6-acetamido-3-(N-(2-(dimethylamino) ethyl) sulfamoyl) naphthalene-1-yl 7-acetamido-4-hydroxynaphthalene-2-sulfonate and its characterization with 1D and 2D NMR techniques

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Indexed by:Journal Article

Date of Publication:2013-07-01

Journal:MAGNETIC RESONANCE IN CHEMISTRY

Included Journals:Scopus、PubMed、SCIE

Volume:51

Issue:7

Page Number:431-434

ISSN:0749-1581

Key Words:NMR; 1 H NMR; 13C NMR; 2D NMR; synthesis

Abstract:A one-step method was reported for the synthesis of 6-acetamido-3-(N-(2-(dimethylamino) ethyl) sulfamoyl) naphthalene-1-yl 7-acetamido-4-hydroxynaphthalene-2-sulfonate by treating 7-acetamido-4-hydroxy-2-naphthalenesulfonyl chloride with equal moles of N, N-dimethylethylenediamine in acetonitrile in the presence of K2CO3. The chemical structure of the obtained compounds was characterized by MS, FTIR, 1H NMR, 13C NMR, gCOSY, TOCSY, gHSQC, and gHMBC. The chemical shift differences of 1H and 13C being 0.04 and 0.2, respectively, were unambiguously differentiated. Copyright (c) 2013 John Wiley & Sons, Ltd.

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