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性别: 男

毕业院校: 大连理工大学

学位: 博士

所在单位: 材料科学与工程学院

联系方式: 0411-84706183

电子邮箱: zxgwj@dlut.edu.cn

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Preparation of diamond nanocrystals from catalysed carbon black in a high magnetic field

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论文类型: 期刊论文

发表时间: 2003-11-26

发表刊物: JOURNAL OF PHYSICS-CONDENSED MATTER

收录刊物: Scopus、SCIE、EI

卷号: 15

期号: 46

页面范围: 8049-8054

ISSN号: 0953-8984

摘要: Under a static high magnetic field of 10 T, diamond-like carbon (DLC) nanocrystals and graphite-coated n-diamond nanoparticles have been synthesized after a pyrogenation of carbon black and a nanometre-sized iron catalyst at atmospheric pressure and a temperature of 1100degreesC. The product is analysed by x-ray diffraction, Raman spectroscopy, transmission electron microscopy and electron-probe microanalysis. The average size of the DLC nanopowders is about 20 nm, and that of the graphite-coated n-diamond particles is about 100 nm. The yield of diamond is as high as 30%.

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